By H. Jäger (auth.), E. L. Grove (eds.)

From the 1st visual appeal of the vintage The Spectrum research in 1885 to the current the sector of emission spectroscopy has been evolving and altering. over the past 20 to 30 years specifically there was an explosion of latest principles and advancements. Of past due, the air of secrecy of glamour has supposedly been transferred to different options, yet, however, it really is anticipated that seventy five% or extra of the analyses performed by way of the steel are entire through emission spectroscopy. extra, the superb sensitivity of plasma resources has created a requirement for this method in such divergent parts as direct hint point analyses in polluted waters. advancements within the replication method and advances within the paintings of professional­ ducing governed and holographic gratings in addition to advancements within the fabrics from which those gratings are made have made first-class gratings on hand at average costs. This availability and the improvement of airplane grating mounts have contributed to the expanding approval for grating spectrometers as com­ pared with the big prism spectrograph and concave grating mounts. different parts of development contain new and better equipment for excitation, using managed atmospheres and the extension of spectrometry into the vacuum quarter, the frequent program of the concepts for research of nonmetals in metals, the expanding use of polychrometers with concave or echelle gratings and more desirable readout platforms for higher examining of spectrographic plates and extra effective facts handling.

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Acta 58,51 (1972). 78. H. Jiiger, Anal. Chim. Acta 71, 43 (1974). 79. H. Jager, Anal. Chim. Acta 60, 303 (1972). 46 CHAPTER 1 80. R. M. Lowe, Spectrochim. Acta 31B, 257 (1976). 81. E. Manrique, Methods for Emission Spectrochemical Analysis, American Society for Testing and Materials, Philadelphia (1971), p. 639. 82. E. Jackwerth, G. Graffmann, and J. Lohmar, Z. Anal. Chern. 247, 149 (1969). 83. B. M. Talalev, Zh. Anal. Khim. 12, 1443 (1966). 84. L. K. Larina, N. S. Belenkova, and N. F. Sachkova, Zh.

10 Determination of Noble Metals in Various Materials, Graphite Electrode Technique :I: :0 m -t ""0 )> (") ~ PRECIOUS METALS 21 Balfour et al.

89) Copper is converted into copper oxide by roasting. Sample pellets are melted into buttons in the crater of the positive electrode of a de arc and then excited after changing the polarity. 11 summarizes these methods. 3 Other Methods Goleb, in two publications, described the determination of ruthenium, rhodium, palladium, and other elements in uranium fission alloys. <90• 91) The first of the references deals with the point-to-plane technique , and the second with a water-cooled hollow cathode lamp.

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